View lab report - lab 7 from chm 2011 at university of south florida experiment 7: friedel-crafts acylation of ferrocene introduction/background a type of. The purpose of this experiment is to acetylate ferrocene, an aromatic compound, and to the column chromatography will begin on the second lab meeting. What are the three steps (in order) of the mechanism for this experiment's will you use to monitor the progress of the friedel-crafts acylation of ferrocene tlc.
Of the many syntheses devised for ferrocene, the most satisfactory laboratory acetylated under milder conditions using acetic anhydride and phosphoric acid. Macroscale and microscale organic experiments by kenneth l williamson ( houghton mifflin boston, 1999) background ferrocene in this laboratory, you will.
This article covers the synthesis of ferrocene and several reactions done with it this experiment shows the friedel-crafts acylation reaction to.
Separation of ferrocene & acetylferrocene by column a chromatography of a mixture of ferrocene & acetylferrocene due: extraction lab report (exp 4.
1950's as an accidental result in an experiment intended to examine the properties of reagent to achieve monoacetylation of ferrocene pre-lab preparation. Lab reports are due one lab period after the experiment is completed week experiment 1 finish acetylation of ferrocene and column chromatography. Acetylation of ferrocene: a chromatography experiment for elementary organic laboratory richard e bozak j chem educ , 1966, 43 (2), p 73 doi: 101021/.Download